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Fluoronickelate

The fluoronickelates are a class of chemical compounds containing an anion with nickel at its core, surrounded by fluoride ions which act as ligands. The nickel atom can be in a range of oxidation states from +2, +3 to +4. The hexafluoronickelate(IV) ion NiF contains nickel in the maximal +4 state, and is octahedral coordination by the fluoride atoms. It forms a commercially available salt Potassium hexafluoronickelate(IV) KNiF. Solid double salts can contain tetrafluoronickelate NiF eg KNiF.

formula

name

Ni Ox

structure

Remarks

references

(NH)NiF

ammonium tetrafluoronickelate

2

Fuse NiCl with NHF

(NH)NiF·2HO

ammonium tetrafluoronickelate dihydrate

2

Formed from Ni(OH) and NHF in water

KNiF

potassium tetrafluoronickelate

2

RbNiF

rubidium tetrafluoronickelate

2

BaNiF

barium nickel fluoride

2

yellow square plates cas=18115-49-6

PbNiF

lead(II)nickel(II) fluoride

2

cas=27037-78-1

LiNiF

3

Pna2 C a=9.60 Å b=8.37 Å c=4.09 Å Z=4 density=3.27 / 3.24

formed at at 500° 70 bar F

NaNiF

sodium hexafluoronickelate

3

violet cas=22707-99-9

KNiF

potassium hexafluoronickelate

3

violet cas=14881-07-3

KCsNiF

dicesium potassium hexafluoronickelate

3

lilac colour cas=53479-35-9

LiNiF

lithium hexafluoronickelate

4

hexagonal a=8.321 Å c=4.598 Å V=275.7 Å Z=3

pink sol 0.5 g/100 g HF at 0°

(O)NiF

dioxygenyl hexafluoronickelate

possibly existing, decompose 10°

(NO)NiF

dinitronium hexafluoronickelate

4

ΔH=-471 kJ/mol, ΔH=-1120

NaNiF

sodium hexafluoronickelate

4

cubic; or tetragonal

purple red

KNiF

potassium hexafluoronickelate

4

KPtCl structure

red cas=17218-47-2

CaNiF

calcium hexafluoronickelate

4

ΔH=-363 kJ/mol, ΔH=-1951 kJ/mol sold as a fluorine source

RbNiF

rubidium hexafluoronickelate

4

KPtCl structure

red cas=17218-48-3

CsNiF

Cesium hexafluoronickelate

4

KPtCl structure

red cas=17218-49-4

SrNiF

strontium hexafluoronickelate

4

red cas=66456-12-0

BaNiF

barium hexafluoronickelate

4

KPtCl structure

red cas=66456-13-1

(NF)NiF

bis-tetrafluoroammonium hexafluoronickelate

4

tetragonal KPtCl structure

red cas=63105-40-8

(ClFO)NiF

bis [difluorooxychlorine (V)] hexafluoronickelate (IV)

4

deep purple, stable to 60°C